Publications 2019–2020


257. Accelerating Electrochemical Synthesis through Automated Flow: Efficient Synthesis of Chalcogenophosphites
N. Amri, T. Wirth, Synlett 2020, 31, 1894–1898. DOI

256. Accelerating biphasic biocatalysis through new process windows
F. Huynh, M. Tailby, A. Finniear, K. Stephens, R. K. Allemann, T. Wirth, Angew. Chem. 2020132, 16632–16637; DOI  Angew. Chem. Int. Ed. 2020, 59, 16490–16495. DOI

255. Selective hydroboration – oxidation of terminal alkenes under flow conditions
M. Elsherbini, F. Huynh, A. Dunbabin, R. K. Allemann, T. Wirth, Chem. Eur. J. 202026, 11423–11425. DOI Highlighted in Synfacts

254. Hypervalent Iodine(III)-Catalysed Enantioselective α-Acetoxylation of Ketones
T. Hokamp, T. Wirth, Chem. Eur. J. 202026, 10417–10421. DOI

253. Short Total Synthesis of Ajoene, (E,Z)-4,5,9-Trithiadodeca-1,6,11-triene 9-oxide, in Batch and (E,Z)-4,5,9-Trithiadodeca-1,7,11-triene in Continuous Flow
M. Yamamoto Raynbird, F. Silva, H. Smallman, S. S. Khokhar, D. Neef, G. J. S. Evans, T. Wirth, Chem. Eur. J. 202026, 8363–8367. DOI

252. Automated Electrochemical Selenenylations
N. Amri, T. Wirth, Synthesis 2020, 52, 1751–1761. DOI

251. Immobilised Enzymes for Sesquiterpene Synthesis in Batch and Flow Systems
D. Valikhani, P. L. Srivastava, R. K. Allemann, T. Wirth, ChemCatChem 2020, 12, 2194–2197. DOI

250. 1,3-Carboboration of Iodonium Ylides
T. A. Gazis, B. A. Mohajeri, D. Willcox, D. M. C. Ould, J. Wenz, J. M. Rawson, M. S. Hill, T. Wirth, R. L. Melen, Chem. Commun. 2020, 56, 3345–3348. DOI


249. Memory of Chirality in Flow Electrochemistry: Fast Optimisation with DoE and Online 2D-HPLC
M. Santi, J. Seitz, R. Cicala, T. Hardwick, N. Ahmed, T. Wirth, Chem. Eur. J. 201925, 16230–16235. DOI

248. Electroorganic Synthesis under Flow Conditions
M. Elsherbini, T. Wirth, Acc. Chem. Res. 2019, 52, 3287–3296. DOI

247. Manganese-Catalyzed Electrochemical Deconstructive Chlorination of Cycloalkanols via Alkoxy Radicals
B. D. W. Allen, M. D. Hareram, A. C. Seastram, T. McBride, T. Wirth, D. L. Browne, L. C. Morrill, Org. Lett. 2019, 21, 9241–9246. DOI

246. Electrochemistry under Flow Conditions
A. A. Folgueiras-Amador, T. Wirth in Flow Chemistry: Integrated Approaches for Practical Applications, Eds: S. V. Luis, E. Garcia-Verdugo, RSC Publishing, 2019, pp. 153–198. DOI

245. ‘Dark’ Singlet Oxygen Made Easy
M. Elsherbini, R. K. Allemann, T. Wirth, Chem. Eur. J. 201925, 12486–12490. DOI Highlighted in OPRD

244. Reactions of hydrazones and hydrazides with Lewis acidic boranes
T. A. Gazis, A. Dasgupta, M. S. Hill, J. M. Rawson, T. Wirth, R. L. Melen, Dalton Trans. 2019, 48, 12391–12395. DOI

243. Synthesis, characterisation, and reactivity of novel pseudocyclic hypervalent iodine reagents with heteroaryl carbonyl substituents
J. Qurban, M. Elsherbini, H. Alharbi, T. Wirth, Chem. Commun. 2019, 55, 7998–8000. DOI

242. Structurally Defined α-Tetralol-Based Chiral Hypervalent Iodine Reagents
T. Hokamp, T. Wirth, J. Org. Chem. 2019, 84, 8674–8682. DOI

241. Continuous Flow Electrochemical Generator of Hypervalent Iodine Reagents: Synthetic Applications
M. Elsherbini, B. Winterson, H. Alharbi, A. A. Folgueiras-Amador, C. Génot, T. Wirth, Angew. Chem. 2019131, 9916-9920; DOI  Angew. Chem. Int. Ed. 2019, 58, 9811–9815. DOI Highlighted in Synfacts

240. 2-Iodoxybenzoic acid ditriflate: the most powerful hypervalent iodine(V) oxidant
M. S. Yusubov, N. S. Soldatova, P. Postnikov, R. R. Valiev, A. Yoshimura, T. Wirth, V. Nemykin, V. V. Zhdankin, Chem. Commun. 2019, 55, 7760–7763. DOI  Highlighted in Chemistry World

239. Efficient Flow Electrochemical Alkoxylation of Pyrrolidine-1-carbaldehyde
N. Amri, R. A. Skilton, D. Guthrie, T. Wirth, Synlett 201930, 1183–1186. DOI

238. Metal-Free Tandem Rearrangement/Lactonization: Access to 3,3-Disubstituted Benzofuran-2-(3H)-ones
M. Santi, D. M. C. Ould, J. Wenz, Y. Soltani, R. L. Melen, T. Wirth, Angew. Chem. 2019131, 7943–7947; DOI Angew. Chem. Int. Ed. 2019, 58, 7861–7865. DOI

237. Morpholin-2-one Derivatives via Intramolecular Acid-Catalyzed Hydroamination
A. H. Aldimairi, D. W. Knight, T. Wirth, Synthesis 2019, 51, 1643–1648. DOI

236. Flow Synthesis of Iodonium Trifluoroacetates through Direct Oxidation of Iodoarenes by Oxone®
N. S. Soldatova, P. S. Postnikov, M. S. Yusubov, T. Wirth, Eur. J. Org. Chem. 2019, 2081–2088. DOI

235. Meet the Board of ChemistryOpen: Thomas Wirth
T. Wirth, ChemistryOpen 2019, 8, 251. DOI

234. Selenium Reagents as Catalysts
F. V. Singh, T. Wirth, Catal. Sci. Technol. 2019, 9, 1073–1091. DOI

233. Efficient Electrosynthesis of Thiazolidin-2-imines via Oxysulfurization of Thiourea-Tethered Terminal Alkenes using the Flow Microreactor
M. Islam, B. M. Kariuki, Z. Shafiq, T. Wirth, N. Ahmed, Eur. J. Org. Chem. 2019, 1371–1376. DOI

232. Selenium and Tellurium Electrophiles in Organic Synthesis
F. V. Singh, T. Wirth in Selenium and Tellurium Reagents, Eds. R. Laitinen, R. Oilunkaniemi, De Gruyter, 2019, pp. 243–299.
F. V. Singh, T. Wirth, Phys. Sci. Rev. 2019, 4. DOI

231. Enantioselective Electrochemical Lactonization Using Chiral Iodoarenes as Mediators
W.-C. Gao, Z.-Y. Xiong, S. Pirhaghani, T. Wirth, Synthesis 2019, 51, 276–284. DOIoa