Publications 2018–2019

2019

249. Memory of Chirality in Flow Electrochemistry: Fast Optimisation with DoE and Online 2D-HPLC
M. Santi, J. Seitz, R. Cicala, T. Hardwick, N. Ahmed, T. Wirth, Chem. Eur. J. 201925in press. DOI

248. Electroorganic Synthesis under Flow Conditions
M. Elsherbini, T. Wirth, Acc. Chem. Res. 2019, in press. DOI

247. Manganese-Catalyzed Electrochemical Deconstructive Chlorination of Cycloalkanols via Alkoxy Radicals
B. D. W. Allen, M. D. Hareram, A. C. Seastram, T. McBride, T. Wirth, D. L. Browne, L. C. Morrill, Org. Lett. 2019, 21, 9241-9246. DOI

246. Electrochemistry under Flow Conditions
A. A. Folgueiras-Amador, T. Wirth in Flow Chemistry: Integrated Approaches for Practical Applications, Eds: S. V. Luis, E. Garcia-Verdugo, RSC Publishing, 2019, pp. 153-198. DOI

245. ‘Dark’ Singlet Oxygen Made Easy
M. Elsherbini, R. K. Allemann, T. Wirth, Chem. Eur. J. 201925, 12486-12490. DOI Highlighted in OPRD

244. Reactions of hydrazones and hydrazides with Lewis acidic boranes
T. A. Gazis, A. Dasgupta, M. S. Hill, J. M. Rawson, T. Wirth, R. L. Melen, Dalton Trans. 2019, 48, 12391-12395. DOI

243. Synthesis, characterisation, and reactivity of novel pseudocyclic hypervalent iodine reagents with heteroaryl carbonyl substituents
J. Qurban, M. Elsherbini, H. Alharbi, T. Wirth, Chem. Commun. 2019, 55, 7998-8000. DOI

242. Structurally Defined α-Tetralol-Based Chiral Hypervalent Iodine Reagents
T. Hokamp, T. Wirth, J. Org. Chem. 2019, 84, 8674-8682. DOI

241. Continuous Flow Electrochemical Generator of Hypervalent Iodine Reagents: Synthetic Applications
M. Elsherbini, B. Winterson, H. Alharbi, A. A. Folgueiras-Amador, C. Génot, T. Wirth, Angew. Chem. 2019131, 9916-9920; DOI  Angew. Chem. Int. Ed. 2019, 58, 9811-9815. DOI Highlighted in Synfacts

240. 2-Iodoxybenzoic acid ditriflate: the most powerful hypervalent iodine(V) oxidant
M. S. Yusubov, N. S. Soldatova, P. Postnikov, R. R. Valiev, A. Yoshimura, T. Wirth, V. Nemykin, V. V. Zhdankin, Chem. Commun. 2019, 55, 7760-7763. DOI  Highlighted in Chemistry World

239. Efficient Flow Electrochemical Alkoxylation of Pyrrolidine-1-carbaldehyde
N. Amri, R. A. Skilton, D. Guthrie, T. Wirth, Synlett 201930, 1183-1186. DOI

238. Metal-Free Tandem Rearrangement/Lactonization: Access to 3,3-Disubstituted Benzofuran-2-(3H)-ones
M. Santi, D. M. C. Ould, J. Wenz, Y. Soltani, R. L. Melen, T. Wirth, Angew. Chem. 2019131, 7943-7947; DOI Angew. Chem. Int. Ed. 2019, 58, 7861-7865. DOI

237. Morpholin-2-one Derivatives via Intramolecular Acid-Catalyzed Hydroamination
A. H. Aldimairi, D. W. Knight, T. Wirth, Synthesis 2019, 51, 1643-1648. DOI

236. Flow Synthesis of Iodonium Trifluoroacetates through Direct Oxidation of Iodoarenes by Oxone®
N. S. Soldatova, P. S. Postnikov, M. S. Yusubov, T. Wirth, Eur. J. Org. Chem. 2019, 2081-2088. DOI

235. Meet the Board of ChemistryOpen: Thomas Wirth
T. Wirth, ChemistryOpen 2019, 8, 251. DOI

234. Selenium Reagents as Catalysts
F. V. Singh, T. Wirth, Catal. Sci. Technol. 2019, 9, 1073-1091. DOI

233. Efficient Electrosynthesis of Thiazolidin-2-imines via Oxysulfurization of Thiourea-Tethered Terminal Alkenes using the Flow Microreactor
M. Islam, B. M. Kariuki, Z. Shafiq, T. Wirth, N. Ahmed, Eur. J. Org. Chem. 2019, 1371-1376. DOI

232. Selenium and Tellurium Electrophiles in Organic Synthesis
F. V. Singh, T. Wirth in Selenium and Tellurium Reagents, Eds. R. Laitinen, R. Oilunkaniemi, De Gruyter, 2019, pp. 243-299.
F. V. Singh, T. Wirth, Phys. Sci. Rev. 2019, 4. DOI

231. Enantioselective Electrochemical Lactonization Using Chiral Iodoarenes as Mediators
W.-C. Gao, Z.-Y. Xiong, S. Pirhaghani, T. Wirth, Synthesis 2019, 51, 276-284. DOIoa

2018

230. Organoselenium Chemistry
F. V. Singh, T. Wirth, in Encyclopedia of Inorganic and Bioinorganic Chemistry, John Wiley & Sons, Ltd: Chichester,  2018. DOI

229. Electrosynthesis in Continuous Flow
A. A. Folgueiras-Amador, T. Wirth, Science of Synthesis, Flow Chemistry in Organic Synthesis, 2018, 147-189. DOI

228. Short Total Synthesis of Ajoene
F. Silva, S. S. Khokhar, D. M. Williams, R. Saunders, G. J. S. Evans, M. Graz, T. Wirth, Angew. Chem. 2018130, 12470-12473; DOI Angew. Chem. Int. Ed. 2018, 57, 12290-12293. DOIoa

227. Hypervalent Iodine Reagents by Anodic Oxidation: a Powerful Green Synthesis
M. Elsherbini, T. Wirth, Chem. Eur. J. 2018, 24, 13399-13407. DOI

226. Preparation and X-ray structure of 2-iodoxybenzenesulfonic acid (IBS) – a powerful hypervalent iodine(V) oxidant
I. A. Mironova, P. S. Postnikov, R. Y. Yusubova, A. Yoshimura, T. Wirth, V. V. Zhdankin, V. N. Nemykin, M. S. Yusubov, Beilstein J. Org. Chem. 2018, 14, 1854-1858. DOIoa

225. Stereoselective reactions
F. V. Singh, T. Wirth, in Patai’s Chemistry of Functional Groups, The Chemistry of Hypervalent Halogen Compounds , Eds. I. Marek, B. Olofsson, Z. Rappoport, John Wiley & Sons, Ltd: Chichester,  2018. DOI

224. Safe use of Hazardous Chemicals in Flow
Md T. Rahman, T. Wirth, Top. Heterocycl. Chem. 2018, 56, 343-373. DOI

223. Alternative Strategies with Iodine: Fast Access to Previously Inaccessible Iodine(III) Compounds
T. Hokamp, L. Mollari, L. C. Wilkins, R. L. Melen, T. Wirth, Angew. Chem. 2018130, 8438-8442; DOI Angew. Chem. Int. Ed. 2018, 57, 8306 -8309. DOI

222. Mechanochemical Synthesis of N-tert-Butanesulfinyl Imines Under Metal-Free Conditions
M. Elsherbini, T. Wirth, Tetrahedron 2018, 74, 3101-3106. DOI

221. Selective Oxidation of Sulfides in Flow Chemistry
F. Silva, A. Baker, J. Stansall, W. Michalska, M. S. Yusubov, M. Graz, R. Saunders, G. J. S. Evans, T. Wirth, Eur. J. Org. Chem. 2018, 2134-2137. DOI

220. Concise Synthesis of Artemisinin from a Farnesyl Diphosphate Analogue
X. Tang, M. Demiray, R. K. Allemann, T. Wirth, Bioorg. Med. Chem. 2018, 26, 1314-1319. DOI

219. One-pot synthesis of diaryliodonium salts from arenes and aryl iodides with Oxone–sulfuric acid
N. Soldatova, P. Postnikov, O. Kukurina, V. V. Zhdankin, A. Yoshimura, T. Wirth, M. S. Yusubov, Beilstein J. Org. Chem. 2018, 14, 849-855. DOIoa

218. Iodine Monoacetate for Efficient Oxyiodinations of Alkenes and Alkynes
T. Hokamp, A. T. Storm, M. Yusubov, T. Wirth, Synlett 2018, 29, 415-418. DOI

217. Reactions of 1-Arylbenziodoxolones with Azide Anion: Experimental and Computational Study of Substituent Effects
M. S. Yusubov, N. S. Soldatova, P. S. Postnikov, R. R. Valiev, D. Y. Svitich, R. Y. Yusubova, A. Yoshimura, T. Wirth, V. V. Zhdankin, Eur. J. Org. Chem. 2018, 640-647. DOI

216. Catalyst- and Supporting Electrolyte-Free Electrosynthesis of Benzothiazoles and Thiazolopyridines in Continuous Flow
A. A. Folgueiras-Amador, X.-Y. Qian, H.-C. Xu, T. Wirth, Chem. Eur. J. 2018, 24, 487-491. DOI Highlighted in Synfacts

215. Synthesis of Organoselenium Compounds with Potential Biological Activities
F. V. Singh, T. Wirth, in Organoselenium Compounds in Biology and Medicine: Synthesis, Biological and Therapeutic Treatments, Eds. V. K. Jain, K. I. Priyadarsini, The Royal Society of Chemistry, 2018, 77-121.